Suchergebnisse - Optimisation and validation of analytical method

Volatile composition of Merlot red wine and its contribution to the aroma: optimization and validation of analytical method von Arcari, Stefany Grützmann, Caliari, Vinicius, Sganzerla, Marla, Godoy, Helena Teixeira

“… ) was developed, validated and applied to a sample of Brazilian red wine. The optimization strategy was conducted using the Plackett-Burman design for variable selection and central composite rotational design (CCRD …”
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Optimisation and validation of a specific analytical method for the determination of thiram residues in fruits and vegetables by LC–MS/MS von Peruga, Aranzazu, Grimalt, Susana, López, Francisco J., Sancho, Juan V., Hernández, Félix

“… ► Specific analytical methodology is developed for determination of dithiocarbamate fungicide thiram in fruits and vegetables …”
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Optimisation and validation of analytical methods for the simultaneous extraction of antioxidants: Application to the analysis of tomato sauces von Motilva, Maria-José, Macià, Alba, Romero, Maria-Paz, Labrador, Agustín, Domínguez, Alba, Peiró, Lluís

“… •Simultaneous extraction of different antioxidants from tomato sauces.•Method for determining antioxidants in tomato sauces is presented and validated.•UPLC …”
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Optimization and validation of an analytical method for the determination of fifteen sweeteners in diabetic foods by HPLC–MS/MS von Rong, Shifan, Shao, Ning, Zou, Peng, Zhu, Dongliang, Zhang, Cheng, Zhu, Xiaolan

“… [Display omitted] •A rapid and sensitive HPLC-MS/MS method was developed to simultaneously determine 7 natural and 8 artificial sweeteners …”
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Maize (Zea mays L.) and mycotoxins: A review on optimization and validation of analytical methods by liquid chromatography coupled to mass spectrometry von Leite, Marta, Freitas, Andreia, Silva, Ana Sanches, Barbosa, Jorge, Ramos, Fernando

“… Mycotoxins are natural contaminants produced by fungal species that colonize and contaminate crops, in special cereals, either in the field or in post-harvest …”
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Biogenic amines and their metabolites in mouse brain tissue: Development, optimization and validation of an analytical HPLC method von Nguyen, A.T., Aerts, T., Van Dam, D., De Deyn, P.P.

“… A simple and fast HPLC method based on an isocratic, reversed-phased ion-pair with amperometric end-point detection for simultaneous measurement of noradrenergic (MHPG/NA and A), dopaminergic (DOPAC, HVA/DA) and serotonergic (5-HIAA/5-HT …”
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Presence of parabens in children’s faeces. Optimization and validation of a new analytical method based on the use of ultrasound-assisted extraction and liquid chromatography-tandem mass spectrometry von Moscoso-Ruiz, Inmaculada, Navalón, Alberto, Rivas, Ana, Zafra-Gómez, Alberto

“… A new analytical method has been optimised and validated. The method …”
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Box–Behnken design aided optimization and validation of developed reverse phase HPLC analytical method for simultaneous quantification of dolutegravir sodium and lamivudine co‐loaded in nano‐liposomes von Mutalik, Sadhana P, Mullick, Prashansha, Pandey, Abhijeet, Kulkarni, Smita S., Mutalik, Srinivas

“… A stability‐indicating reversed‐phase high‐performance liquid chromatography method for simultaneous estimation of dolutegravir sodium and lamivudine encapsulated in the nanoliposomal formulation was developed …”
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Validation and optimisation of reduced glutathione quantification in erythrocytes by means of a coulometric high‐performance liquid chromatography analytical method von Lauwers, Stef, Van Herreweghe, Maxim, Foubert, Kenn, Theunis, Mart, Breynaert, Annelies, Tuenter, Emmy, Hermans, Nina

“… This paper provides a sensitive analytical method using HPLC‐ECD to quantify GSH in erythrocytes, validated using the ICH guidelines for Bioanalytical Method Validation …”
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Optimization and Validation of an Analytical Method for the Determination of Sweeteners in Beverages by HPLC-ELSD von de Sousa, Roberto Cesar Santos, de Fatima Gomides, Maria, Costa, Karen, Ribeiro Cunha, Mariem R., de Oliveira Almeida, Mariana, Custódio, Flavia B., Gloria, Maria Beatriz A.

“… ) followed by an HPLC–ELSD analysis. Validation steps included regression of the analytical curve, recovery, repeatability, and intermediate precision …”
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Determination of total iodine in serum and urine samples by ion chromatography with pulsed amperometric detection – Studies on analyte loss, optimization of sample preparation procedures, and validation of analytical method von Błażewicz, Anna, Klatka, Maria, Dolliver, Wojciech, Kocjan, Ryszard

“… •Optimization of various sample preparation procedures was carried out.•Recovery was higher with alkaline than acidic digestion followed by ammonification …”
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Optimization and validation of an analytical method for the quantification of short- and medium-chained chlorinated paraffins in food by gas chromatography-mass spectrometry von McGrath, Thomas J., Poma, Giulia, Bombeke, Jasper, Limonier, Franck, Van Hoeck, Els, Joly, Laure, Covaci, Adrian

“… This work describes the optimization and validation of an analytical method for the quantification of short- and medium-chained chlorinated paraffins …”
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Determination of proline in honey: Comparison between official methods, optimization and validation of the analytical methodology von Truzzi, Cristina, Annibaldi, Anna, Illuminati, Silvia, Finale, Carolina, Scarponi, Giuseppe

“… •The AOAC method proves to be the best in terms of accuracy and of time-saving.•Optimization of the waiting time for absorbance recording.•Method validation: LOD 20mgkg−1, LOQ 61 mgkg …”
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Rheology of Complex Topical Formulations: An Analytical Quality by Design Approach to Method Optimization and Validation von Chiarentin, Lucas, Cardoso, Catarina, Miranda, Margarida, Vitorino, Carla

“… Analytical method validation ensures that a method provides trustworthy information about a particular sample when applied in accordance with the predefined protocol …”
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ANALYTICAL METHOD OPTIMIZATION AND VALIDATION OF GLIBENCLAMIDE AND METFORMIN HYDROCHLORIDE IN DIABETIC HERBS PRODUCT BY THIN-LAYER CHROMATOGRAPHY-DENSITOMETRY von MAGGADANI, BAITHA PALANGGATAN, SUGIANTO, NOVIANI, HAYUN

“… Objective: This study aimed to develop and validate an analytical method using thin-layer chromatography (TLC …”
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Speciation analysis of organoarsenic species in marine samples: method optimization using fractional factorial design and method validation von Tibon, Jojo, Silva, Marta, Sloth, Jens J., Amlund, Heidi, Sele, Veronika

“… ), making it difficult to evaluate the accuracy of analytical methods for other organoarsenic species …”
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Analytical Method Validation and Formula Optimization of Topical Nanoemulsion Formulation Containing Resveratrol von Nastiti, Christofori Maria Ratna Rini, Riswanto, Florentinus Dika Octa

“… A reversed-phase HPLC method was developed and validated prior to the load determination of RSV in the nanoemulsion formulation …”
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Optimization and validation of an analytical method for the estimation of methotrexate in rabbit plasma von Hussain, Hafiz Rashid, Bashir, Sajid, Khan, Daulat Haleem, Shahzadi, Irum, Rashid, Sheikh Abdur, Khan, Muhammad Hashim, Abdullah, Zaineb, Mahmood, Asif, Sarfraz, Muhammad

“… Analysis was carried out at ʎ max 303 nm and retention time of MTX was found 5.32 min. During the method development and validation ICHQ2 (R1 …”
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A REVIEW ON ANALYTICAL METHOD DEVELOPMENT, OPTIMIZATION AND VALIDATION OF AMLODIPINE AND CELECOXIBBY RP-HPLC von ogeshwari, T, VijeyAanandhi, M, AanandhiProfessorandHead, M Vijey

“… HPLC is an analytical method and key tool for the drug separation, drug quality, monitoring of drugs and in the research of life science …”
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Development, optimization and validation of an analytical method for the determination of voriconazole in plasma by high-performance liquid chromatography-ultraviolet detection: Application for comprehensive study von Berriri, Sarra, Zribi, Kaouther, Gloulou, Olfa, Mokni, Yassine, Safta, Fathi

“… Thus, in this study, we aimed to develop a simple, fast, and efficient method for the determination of voriconazole in plasma using reversed-phase HPLC-UV …”
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