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Compatibility of Kraft Lignin and Phenol-Organosolv Lignin with PLA in 3D Printing and Assessment of Mechanical Recycling

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Název: Compatibility of Kraft Lignin and Phenol-Organosolv Lignin with PLA in 3D Printing and Assessment of Mechanical Recycling
Autoři: Frasca, Serena, Katsiotis, Christos S., Henrik-Klemens, Åke, 1990, Larsson, Anette, 1966, Strømme, Maria, Lindh, Jonas, Galkin, Maxim V., Gising, Johan
Zdroj: Design for Circularity: Lignocellulose based Thermoplastics - Fib:Re ACS Applied Polymer Materials. 6(22):13574-13584
Témata: lignin, poly(lactic acid), blends, biobased materials, recycling
Popis: Lignin is an aromatic biomacromolecule with many promising properties that can be beneficial to polymer blends. The main objective of this work was to investigate the processability, compatibility, and recyclability of lignin blends with poly(lactic acid). Two different commercial kraft lignins and a phenolated organosolv lignin were blended with poly(lactic acid) at various weight percentages, targeting high lignin content (30, 50, and 70 wt %). Obtained blends were used in additive manufacturing via fused deposition modeling. All obtained materials were thoroughly characterized by tensile tests, thermogravimetric analysis, differential scanning calorimetry, and 31P NMR. The recyclability of the polymer blend materials was evaluated by re-extruding them up to four times, and their printability was also assessed. The results showed that the material retained its mechanical properties relatively well for up to three cycles after which its tensile strength decreased by 30%. Phenolated organosolv lignin exhibited better printability across a broader range of lignin content compared to kraft lignin analogs while maintaining similar thermal and mechanical properties.
Popis souboru: electronic
Přístupová URL adresa: https://research.chalmers.se/publication/543735
https://research.chalmers.se/publication/543735/file/543735_Fulltext.pdf
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Items – Name: Title
  Label: Title
  Group: Ti
  Data: Compatibility of Kraft Lignin and Phenol-Organosolv Lignin with PLA in 3D Printing and Assessment of Mechanical Recycling
– Name: Author
  Label: Authors
  Group: Au
  Data: <searchLink fieldCode="AR" term="%22Frasca%2C+Serena%22">Frasca, Serena</searchLink><br /><searchLink fieldCode="AR" term="%22Katsiotis%2C+Christos+S%2E%22">Katsiotis, Christos S.</searchLink><br /><searchLink fieldCode="AR" term="%22Henrik-Klemens%2C+Åke%22">Henrik-Klemens, Åke</searchLink>, 1990<br /><searchLink fieldCode="AR" term="%22Larsson%2C+Anette%22">Larsson, Anette</searchLink>, 1966<br /><searchLink fieldCode="AR" term="%22Strømme%2C+Maria%22">Strømme, Maria</searchLink><br /><searchLink fieldCode="AR" term="%22Lindh%2C+Jonas%22">Lindh, Jonas</searchLink><br /><searchLink fieldCode="AR" term="%22Galkin%2C+Maxim+V%2E%22">Galkin, Maxim V.</searchLink><br /><searchLink fieldCode="AR" term="%22Gising%2C+Johan%22">Gising, Johan</searchLink>
– Name: TitleSource
  Label: Source
  Group: Src
  Data: <i>Design for Circularity: Lignocellulose based Thermoplastics - Fib:Re ACS Applied Polymer Materials</i>. 6(22):13574-13584
– Name: Subject
  Label: Subject Terms
  Group: Su
  Data: <searchLink fieldCode="DE" term="%22lignin%22">lignin</searchLink><br /><searchLink fieldCode="DE" term="%22poly%28lactic+acid%29%22">poly(lactic acid)</searchLink><br /><searchLink fieldCode="DE" term="%22blends%22">blends</searchLink><br /><searchLink fieldCode="DE" term="%22biobased+materials%22">biobased materials</searchLink><br /><searchLink fieldCode="DE" term="%22recycling%22">recycling</searchLink>
– Name: Abstract
  Label: Description
  Group: Ab
  Data: Lignin is an aromatic biomacromolecule with many promising properties that can be beneficial to polymer blends. The main objective of this work was to investigate the processability, compatibility, and recyclability of lignin blends with poly(lactic acid). Two different commercial kraft lignins and a phenolated organosolv lignin were blended with poly(lactic acid) at various weight percentages, targeting high lignin content (30, 50, and 70 wt %). Obtained blends were used in additive manufacturing via fused deposition modeling. All obtained materials were thoroughly characterized by tensile tests, thermogravimetric analysis, differential scanning calorimetry, and 31P NMR. The recyclability of the polymer blend materials was evaluated by re-extruding them up to four times, and their printability was also assessed. The results showed that the material retained its mechanical properties relatively well for up to three cycles after which its tensile strength decreased by 30%. Phenolated organosolv lignin exhibited better printability across a broader range of lignin content compared to kraft lignin analogs while maintaining similar thermal and mechanical properties.
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  Data: electronic
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1021/acsapm.4c02208
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      – Text: English
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        PageCount: 11
        StartPage: 13574
    Subjects:
      – SubjectFull: lignin
        Type: general
      – SubjectFull: poly(lactic acid)
        Type: general
      – SubjectFull: blends
        Type: general
      – SubjectFull: biobased materials
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      – SubjectFull: recycling
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      – TitleFull: Compatibility of Kraft Lignin and Phenol-Organosolv Lignin with PLA in 3D Printing and Assessment of Mechanical Recycling
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            NameFull: Frasca, Serena
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              M: 01
              Type: published
              Y: 2024
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            – TitleFull: Design for Circularity: Lignocellulose based Thermoplastics - Fib:Re ACS Applied Polymer Materials
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