Powder diffraction data of dibromidodioxido-[(4,4′-di-tert-butyl)-2,2′-bipyridine]molybdenum(VI) (C18H24Br2MoN2O2)
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| Názov: | Powder diffraction data of dibromidodioxido-[(4,4′-di-tert-butyl)-2,2′-bipyridine]molybdenum(VI) (C18H24Br2MoN2O2) |
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| Autori: | Julián F. Torrado G., Cristhian C. Álvarez, Oscar Rodríguez B., Jose G. Carriazo, Nelson J. Castellanos |
| Zdroj: | Powder Diffraction. :1-8 |
| Informácie o vydavateľovi: | Cambridge University Press (CUP), 2025. |
| Rok vydania: | 2025 |
| Popis: | This work reports the X-ray powder diffraction (XRPD) data recorded at room temperature (293 K) of dibromidodioxido-[(4,4′-di-tert-butyl)-2,2′-bipyridine]molybdenum(VI). The analysis of the powder diffraction pattern led to an orthorhombic united cell with parameters a = 17.9205(23) Å, b = 13.4451(16) Å, c = 18.1514(19) Å, V = 4,373.5(11) Å3, and values of Z = 8 and Z’ = 2. The crystal structure of this material corresponds to the structure of entry IFUJEC of the Cambridge Structural Database (CSD), determined at 90 K. The excellent Rietveld refinement, carried out with General Structure and Analysis Software II (GSAS-II), showed the single-phase nature of the material and the good quality of the data. This material was also characterized by elemental analysis, UV–vis, Fourier transform infrared spectroscopy (FTIR), and proton nuclear magnetic resonance (1H-NMR) techniques. |
| Druh dokumentu: | Article |
| Jazyk: | English |
| ISSN: | 1945-7413 0885-7156 |
| DOI: | 10.1017/s088571562510078x |
| Rights: | Cambridge Core User Agreement |
| Prístupové číslo: | edsair.doi...........c65ffc5d9672c009063e8feee9bf8cc2 |
| Databáza: | OpenAIRE |
Nájsť tento článok vo Web of Science | Abstrakt: | This work reports the X-ray powder diffraction (XRPD) data recorded at room temperature (293 K) of dibromidodioxido-[(4,4′-di-tert-butyl)-2,2′-bipyridine]molybdenum(VI). The analysis of the powder diffraction pattern led to an orthorhombic united cell with parameters a = 17.9205(23) Å, b = 13.4451(16) Å, c = 18.1514(19) Å, V = 4,373.5(11) Å3, and values of Z = 8 and Z’ = 2. The crystal structure of this material corresponds to the structure of entry IFUJEC of the Cambridge Structural Database (CSD), determined at 90 K. The excellent Rietveld refinement, carried out with General Structure and Analysis Software II (GSAS-II), showed the single-phase nature of the material and the good quality of the data. This material was also characterized by elemental analysis, UV–vis, Fourier transform infrared spectroscopy (FTIR), and proton nuclear magnetic resonance (1H-NMR) techniques. |
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| ISSN: | 19457413 08857156 |
| DOI: | 10.1017/s088571562510078x |