Výsledky vyhledávání - "Synthesis parameters"

Limited influence of externally introduced pressure on the hydrothermal synthesis of V1-xWxO2 (M)

Autoři: Guo, Xinyu Madhav, Dharmjeet Hallez, Hans a další

Přispěvatelé: Guo, Xinyu Madhav, Dharmjeet Hallez, Hans a další

Zdroj: Ceramics International. 51:29240-29247

Témata: Technology, Science & Technology, EFFICIENCY, Materials Science, Vanadium dioxide, PERFORMANCE, Hydrothermal, Synthesis parameters, 34 Chemical sciences, TRANSFORMATION, 09 Engineering, 19 Studies in Creative Arts and Writing, NANORODS, VO2, PHASE-TRANSITION, Interfacial engineering, 36 Creative arts and writing, Energy materials, 03 Chemical Sciences, Materials Science, Ceramics, POLYMORPH, Materials, 40 Engineering

Přístupová URL adresa: https://lirias.kuleuven.be/handle/20.500.12942/765384
https://doi.org/10.1016/j.ceramint.2025.04.130

Unlocking the Full Potential of MgAgSb by Unravelling the Interrelation of Phase Constitution and Thermoelectric Properties

Autoři: Amandine Duparchy Frederic Kreps Eckhard Müller a další

Zdroj: Advanced Functional Materials.

Témata: 'Thermoelectric generators (TEG) focus on harnessing the conversion of heat into electricity, and small (<3 at%), Mg3Sb2 secondary phase appears to be surrounded by cracks, exhibiting high performance from room temperature to 573 K. α-MgAgSb shows attractive thermoelectric (TE) properties and TEG lab prototypes have been successfully fabricated[1], impacting the performance. A long-standing problem of this material system is its sensitivity to minute differences in effective composition and synthesis parameters, resulting in greatly differing TE properties and phase constitution in the micro- and nano-scale. We have investigated MgAgSb samples fabricated by mechanical alloying involving two high energy ball milling runs and two sintering steps. The samples have been synthesized with small differences in synthesis parameters, Thermoelectric generators mechanical properties, holding promise for sustainable energy solutions and space power supply. Magnesium silver antimonide (MgAgSb) stands out among materials, we identified fundamental differences between samples. Depending on synthesis conditions, preventing the development of a microstructure-based understanding of the material properties. By combined microstructural measurements using focused ion beam (FIB) equipped with wavelength dispersive X-ray spectroscopy (WDS), we find a highly dispersed Ag3Sb phase with a typical size < 50 nm throughout some samples, FIB-tomography, most likely influencing the resulting material performance. Analysis of the TE properties employing the Boltzmann formalism reveals strongly varying effective scattering constants depending on secondary phase type and content. Our approach reveals secondary phases to be a key player in this system and sets the foundation for synthesis upscaling and technological maturity of this material.', but its sensitivity to secondary phases poses challenges[2], the employed SEM/EDS and XRD analysis is limited with respect to compositional and spatial resolution, resulting in different effective compositions, invisible to XRD and SEM, which is identified to be highly detrimental to the TE properties. Similarly, scanning transmission electron microscopy with energy-dispersive X-ray spectroscopy (STEM-EDS) and electron diffraction, but varying amount of secondary phases. For those we have found recently a clear correlation between effective composition, the content of secondary phases and the resulting thermoelectric properties[2]. However, Thermoelectric generators TEG convert heat electricity

Přístupová URL adresa: https://elib.dlr.de/211872/
https://elib.dlr.de/211874/
https://elib.dlr.de/211875/

Chemically driven dimensionality modulation of hybrid tin(ii) halide perovskite microcrystals

Autoři: Raúl I. Sánchez-Alarcón Omar E. Solís María Cristina Momblona-Rincon a další

Přispěvatelé: Raúl I. Sánchez-Alarcón Omar E. Solís María Cristina Momblona-Rincon a další

Zdroj: RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Universitat Politècnica de València (UPV)

Témata: Perovskite microcrystals, Three-dimensional counterpart, Synthesis parameters

Popis souboru: application/pdf

Přístupová URL adresa: https://riunet.upv.es/handle/10251/206885
https://hdl.handle.net/10251/206885
https://doi.org/10.1039/d4tc00623b

Comprehensive study of dual-doped TiO2 thin films: Phase transition, bandgap tuning, and microstructural characterization

Autoři: Abhishek Prasad Fouran Singh Vivek Dhuliya a další

Zdroj: Next Materials, Vol 7, Iss , Pp 100632- (2025)

Témata: Hybrid phases, Refractive index, Cr-N doped TiO2, Phase dominance, Synthesis parameters, Transition temperature, Technology

Popis souboru: electronic resource

Relation: http://www.sciencedirect.com/science/article/pii/S2949822825001509; https://doaj.org/toc/2949-8228

Přístupová URL adresa: https://doaj.org/article/335876ccbcea406097cefe9dc41b533f

Tailoring MOF-5 Photocatalysts: Low-Temperature Synthesis and Solvent Variations for Enhanced Performance in Dye Degradation

Autoři: Himanshi Gupta Isha Saini Vinamrita Singh a další

Zdroj: Bulletin of Chemical Reaction Engineering & Catalysis, Vol 19, Iss 1, Pp 1-14 (2024)

Témata: mof-5, synthesis parameters, Chemical engineering, water treatment, TP155-156, 02 engineering and technology, 0210 nano-technology, photocatalysis, organic dye degradation, 01 natural sciences, 0104 chemical sciences

Přístupová URL adresa: https://doaj.org/article/2f6a8a8ceed74ea9a804e40ac4811163

Optimization of Mixed Metal Oxide Electrodes for Chlorine Generation: An Alternative to Conventional Platinum Group Metal Materials

Autoři: Shane M. Hancox Xiaohan Shao Woonghee Lee a další

Témata: Biophysics, Biotechnology, Evolutionary Biology, Science Policy, Chemical Sciences not elsewhere classified, Physical Sciences not elsewhere classified, factorial design study, dilute chloride solutions, analyze electrode composition, agcl ,, co molar ratio, cer ), however, 5 mah charge, electrode surface morphology, >), >, anode surface, sub ><, − 1, widespread adoption, synthesis parameters, synthesis conditions, suitable low, plating solution, neutral ph, material properties, faradaic efficiency, driving factor, conventional ru

Relation: https://figshare.com/articles/journal_contribution/Optimization_of_Mixed_Metal_Oxide_Electrodes_for_Chlorine_Generation_An_Alternative_to_Conventional_Platinum_Group_Metal_Materials/30120203

Dostupnost: https://doi.org/10.1021/acs.est.5c07308.s001
https://figshare.com/articles/journal_contribution/Optimization_of_Mixed_Metal_Oxide_Electrodes_for_Chlorine_Generation_An_Alternative_to_Conventional_Platinum_Group_Metal_Materials/30120203

Stabilization of Vaterite in Nanostructured CaCO 3 via Precipitation: Implications for Drug Delivery Systems

Autoři: M. M. Gonzalez P. E. Di Prátula D. G. Lamas a další

Témata: Biophysics, Biotechnology, Ecology, Chemical Sciences not elsewhere classified, spherical forms , simple organic additives, normal laboratory conditions, least 3 years, human cancer therapies, adjusting synthesis parameters, 35 ° c, 3 , 2 , via precipitation, systematic correlation, stable caco, solution using, resulting batch, remained stable, precipitation routes, polyethylene glycol, nanostructured caco, interesting material, infusion pump, excess reactants, drug delivery, crystallite size, continuous stirring, aggregate morphology, adding cacl

Relation: https://figshare.com/articles/journal_contribution/Stabilization_of_Vaterite_in_Nanostructured_CaCO_sub_3_sub_via_Precipitation_Implications_for_Drug_Delivery_Systems/30117765

Dostupnost: https://doi.org/10.1021/acsanm.5c03001.s001
https://figshare.com/articles/journal_contribution/Stabilization_of_Vaterite_in_Nanostructured_CaCO_sub_3_sub_via_Precipitation_Implications_for_Drug_Delivery_Systems/30117765

Machine Learning-Enabled Prediction of Synthesis–Property Relationships in Cobalt Nanowires as Rare-Earth-Free Permanent Magnets

Autoři: Jie Zhang Zhi Yang Xiaoxiao Zhang a další

Témata: Medicine, Sociology, Space Science, Biological Sciences not elsewhere classified, Information Systems not elsewhere classified, supply chain vulnerabilities, reviewed literature focusing, polyol reduction methods, performance permanent magnets, free permanent magnets, systematic experimental investigations, machine learning insights, machine learning analysis, provides experimental validation, performance cobalt nanowires, machine learning, experimental validation, cobalt nanowires, yet understanding, work demonstrates, synthesis parameters, switching behavior, sustainability associated, reducing agents, rational design, process parameters, nucleating agents, model predictions, magnetic uniformity, enabled prediction

Dostupnost: https://doi.org/10.1021/acsami.5c12123.s001
https://figshare.com/articles/journal_contribution/Machine_Learning-Enabled_Prediction_of_Synthesis_Property_Relationships_in_Cobalt_Nanowires_as_Rare-Earth-Free_Permanent_Magnets/29671295

Co–Mo Catalysts Supported on CNT/H-ZSM‑5 Composites for Selective Production of Sustainable Aviation Fuel-Range Alkanes

Autoři: K. Kaiser Ferreira B. F. Oliveira Magalhães L. Sousa Ribeiro a další

Témata: Biophysics, Biochemistry, Medicine, Ecology, Immunology, Space Science, Chemical Sciences not elsewhere classified, yield hydrocarbons within, sustainable aviation fuel, structural properties tailored, innovative catalytic support, enhancing product selectivity, component catalysts highlighted, combining carbon nanotubes, co – mo, lipid model compound, 16 , systematically investigated, synthesis parameters, subsequently impregnated, selective production, resulting composites, physical mixtures, palmitic acid, optimized textural, milling time, milling process, lipid feedstocks, free ball, findings demonstrate

Dostupnost: https://doi.org/10.1021/acs.energyfuels.5c02344.s001
https://figshare.com/articles/journal_contribution/Co_Mo_Catalysts_Supported_on_CNT_H-ZSM_5_Composites_for_Selective_Production_of_Sustainable_Aviation_Fuel-Range_Alkanes/29594551

Controlling the Hierarchical Morphology of ZIF-67 via Hydrothermal Synthesis: Insights into the Stability for Gas Separation

Autoři: Paula S. Pacheco Sônia Faria Zawadzki Daniel Eiras

Témata: Biophysics, Cell Biology, Ecology, Infectious Diseases, Space Science, Biological Sciences not elsewhere classified, Chemical Sciences not elsewhere classified, promote micelle formation, resulting hierarchical structures, gas separation membranes, 2 , gas separation applications, gas separation, hierarchical morphology, water compared, vigorously stirring, uniform morphology, synthesis parameters, synthesis conditions, study focuses, structural integrity, structural degradation, samples containing, results highlight, primary goal, particularly co, metal precursor, improved crystallinity, hydrothermal method, controlled temperatures

Dostupnost: https://doi.org/10.1021/acs.langmuir.5c01142.s001
https://figshare.com/articles/journal_contribution/Controlling_the_Hierarchical_Morphology_of_ZIF-67_via_Hydrothermal_Synthesis_Insights_into_the_Stability_for_Gas_Separation/29525049

Binder-Free Flexible Anodes Utilizing Nanocellulose-Templated Mesoporous Silica for High-Performance Li-Ion Batteries

Autoři: Nancy Chen Morteza Sabet Kelliann C. Koehler a další

Témata: Biophysics, Biochemistry, Medicine, Biotechnology, Ecology, Inorganic Chemistry, Space Science, Chemical Sciences not elsewhere classified, templated mesoporous silica, optimizing synthesis parameters, free flexible electrodes, environmentally benign approach, conformal carbon layer, c composite nanoparticles, stable cycling performance, performance li, sustainable template, study presents, silicanqs ), ion batteries, conductive network, 200 cycles

Dostupnost: https://doi.org/10.1021/acsaem.5c01508.s001
https://figshare.com/articles/journal_contribution/Binder-Free_Flexible_Anodes_Utilizing_Nanocellulose-Templated_Mesoporous_Silica_for_High-Performance_Li-Ion_Batteries/29446920

Navigating Small Datasets with Machine Learning: Gaussian Process Modeling for Colloidal Gelation

Autoři: Rohan Batra Yogesh M. Joshi Sachin Shanbhag

Témata: Biochemistry, Biological Sciences not elsewhere classified, Mathematical Sciences not elsewhere classified, Information Systems not elsewhere classified, superior uncertainty calibration, simultaneously learn correlations, multiple synthesis pathways, map synthesis parameters, many traditional science, address inverse problems, two different structures, favor multioutput gp, driven framework based, navigating small datasets, gaussian process modeling, small datasets, gp model, gaussian processes, different outputs, bayesian framework, large datasets, work presents, robust methodology, model predictions, material design, machine learning, gelation characteristics, engineering disciplines, constrained modeling, colloidal domain

Relation: https://figshare.com/articles/journal_contribution/Navigating_Small_Datasets_with_Machine_Learning_Gaussian_Process_Modeling_for_Colloidal_Gelation/29355159

Dostupnost: https://doi.org/10.1021/acs.langmuir.5c00754.s001
https://figshare.com/articles/journal_contribution/Navigating_Small_Datasets_with_Machine_Learning_Gaussian_Process_Modeling_for_Colloidal_Gelation/29355159

Engineering ZnAl-LDHs: The Impact of Synthesis Parameters on Material Properties for Adsorption Applications

Autoři: Pollyanna Vanessa dos Santos Lins Rafaela Gabriel Wagner Roberto de Oliveira Pimentel a další

Témata: Biophysics, Microbiology, Biotechnology, Inorganic Chemistry, Chemical Sciences not elsewhere classified, upper level across, experimental analysis indicated, factorial experimental design, 24 h ), 3 , 12 ), time, 11 synthesized materials, 11 materials, reactor design, zero charge, wide variety, synthesized via, synthesis parameters, surface area, study employed, reaction parameters, reaction factors, produce znal, modifying factors, material properties, highest performance, engineering znal, crystallite size, coprecipitation method

Dostupnost: https://doi.org/10.1021/acsaenm.5c00140.s001
https://figshare.com/articles/journal_contribution/Engineering_ZnAl-LDHs_The_Impact_of_Synthesis_Parameters_on_Material_Properties_for_Adsorption_Applications/29245659

Comprehensive Screening of Conditions for Block Copolymer Nanoaggregate Formation via Automated DLS

Autoři: Lakshani J. Weerarathna Oliver Weismantel Tanja Junkers

Témata: Biochemistry, Medicine, Microbiology, Pharmacology, Biotechnology, Sociology, Space Science, Chemical Sciences not elsewhere classified, statistically robust result, overall polymer concentration, organic solvent phase, monitored online via, low polymer concentrations, overall flow rate, methyl ether acrylate, high flow rates, ethyl methacrylate )-<, amphiphilic block copolymer, hydroxy ethyl acrylate, obtainable particle sizes, high water contents, 2 -( dimethylamino, ethyl acrylate, particle sizes, continuous flow, block <, synthesis platform, synthesis parameters, standard deviation, smaller particles

Relation: https://figshare.com/articles/journal_contribution/Comprehensive_Screening_of_Conditions_for_Block_Copolymer_Nanoaggregate_Formation_via_Automated_DLS/29105259

Dostupnost: https://doi.org/10.1021/acs.macromol.4c03171.s001
https://figshare.com/articles/journal_contribution/Comprehensive_Screening_of_Conditions_for_Block_Copolymer_Nanoaggregate_Formation_via_Automated_DLS/29105259

High Yield Au Nanorods Synthesis: Investigation of the Synthesis Parameters Tunability by Statistical Methods

Autoři: Antonin Engel Fabien Drault Sophie Madeleine Demoustier-Champagne a další

Témata: Medicine, Biotechnology, Biological Sciences not elsewhere classified, rod aspect ratio, present study explores, optimal experimental conditions, gold precursor concentrations, mild reducing agent, synthesis parameters tunability, ctab ), hydroquinone, reducing agent, new conditions, gold consumption, web application, two components, statistical analysis, silver nitrate, predictive power, particularly suitable, model designed, medical imaging, mediated method, infrared portion, freely access, customized design, controlled ar, comprehensive understanding, cetyltrimethylammonium bromide, ascorbic acid

Relation: https://figshare.com/articles/journal_contribution/High_Yield_Au_Nanorods_Synthesis_Investigation_of_the_Synthesis_Parameters_Tunability_by_Statistical_Methods/28938412

Dostupnost: https://doi.org/10.1021/acs.langmuir.5c00326.s001
https://figshare.com/articles/journal_contribution/High_Yield_Au_Nanorods_Synthesis_Investigation_of_the_Synthesis_Parameters_Tunability_by_Statistical_Methods/28938412

Aqueous Cymbopogon citratus Extract Mediated Silver Nanoparticles: Part I. Influence of Synthesis Parameters, Characterization, and Biomedical Studies

Autoři: Himabindu Kurra Aditya Velidandi Mounika Sarvepalli a další

Zdroj: Nanomaterials ; Volume 15 ; Issue 5 ; Pages: 328

Témata: biomedical applications, green synthesis, silver nanoparticles, synthesis parameters

Popis souboru: application/pdf

Relation: Synthesis, Interfaces and Nanostructures; https://dx.doi.org/10.3390/nano15050328

Dostupnost: https://doi.org/10.3390/nano15050328

Preparation and regulation of perovskite hydroxide nanomaterials

Autoři: SHAO Jing LONG Xinyi FANG Yusheng a další

Zdroj: Shenzhen Daxue xuebao. Ligong ban, Vol 40, Iss 4, Pp 379-385 (2023)

Témata: Technology, synthesis parameters, co-precipitation method, electrochemical performance, perovskite hydroxides, nanomaterials, micro-morphology

Přístupová URL adresa: https://doaj.org/article/0bb7c2e4a6d84887a5685d492410a0e3

Influence of synthesis parameters on the optical properties of carbon dots

Autoři: Ángela J. García-Salcedo Luz Ángela Giraldo-Pinto Deibys Josué Márquez-Castro a další

Zdroj: Carbon Trends, Vol 17, Iss , Pp 100403- (2024)

Témata: Carbon dots, Hydrothermal treatment, Synthesis parameters, Quantum yield, Photoluminescence, Chemistry, QD1-999

Popis souboru: electronic resource

Relation: http://www.sciencedirect.com/science/article/pii/S2667056924000841; https://doaj.org/toc/2667-0569

Přístupová URL adresa: https://doaj.org/article/866c75b53fec4db7b9d505edf46c080f

Effect of different physical factors on the synthesis of spherical gold nanoparticles towards cost‐effective biomedical applications

Autoři: Zahra Bahmanyar Fatemeh Mohammadi Ahmad Gholami a další

Zdroj: IET Nanobiotechnol
IET Nanobiotechnology, Vol 17, Iss 1, Pp 1-12 (2023)

Témata: synthesis efficacy, Cost-Benefit Analysis, Turkevich method, Metal Nanoparticles, 02 engineering and technology, 01 natural sciences, Citric Acid, 0104 chemical sciences, synthesis parameters, gold nanoparticles, Spectroscopy, Fourier Transform Infrared, synthesis optimization, Gold, 0210 nano-technology, TP248.13-248.65, Biotechnology, Regular Articles

Přístupová URL adresa: https://pubmed.ncbi.nlm.nih.gov/36326590
https://doaj.org/article/25b77f7825404df69c22fe8e41d37eaf

The Effect of Glycine Quantity on the Phase Formation and Crystal Structures of Ce1-xLaxO2 (x=0.04) Nanoparticles Synthesized by Glycine Combustion Technique

Autoři: Kırkgeçit, Nurvet Kırkgeçit, Rabia Kırkgeçit, Ayşe

Zdroj: Volume: 1, Issue: 143-50
KİÜ Fen, Mühendislik ve Teknoloji Dergisi

Témata: Cerium Oxide, Glycine Combustion Technique, Synthesis Parameters, Malzeme Fiziği, Material Physics, Seryum oksit, Glisin yakma tekniği, Sentez parametreleri

Popis souboru: application/pdf

Přístupová URL adresa: https://dergipark.org.tr/tr/pub/kiufemte/issue/84168/1463784