Suchergebnisse - "Mohammad A"

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    Morphology and Physiochemical Characterization of Perfluorosulfonic Acid (PFSA) Membrane forElectrochemical ApplicationMohd Hafiz Md Ali1, Mohammad Noor Jalil1*, Mohamad Nor Amirul Azhar Kamis1,Hamizah Mohd Zaki11School of Chemistry and Environment, Faculty of Applied Science,Universiti Teknologi MARA, Shah Alam, 40000, Selangor MALAYSIA*Corresponding Author: moham423@uitm.edu.myDOI: https://doi.org/10.30880/jst.2025.17.01.011 Article InfoAbstractReceived: 11 September 2024Accepted: 17 May 2025 Available online: 30 June 2025This reportprovides a thorough examination of the surface morphology, chemical content, and physical properties of Perfluorosulfonic Acid (PFSA) membrane which is commonly utilised as a conductive membrane in fuel cells, ionic batteries, and electrolysers. This experimental effort is separated into two parts: morphological characterisation and physicochemical analysis, which aim to improve understanding of the membrane functional qualities. The membrane surface and cross-sectional characteristics were examined at varied magnifications using Field Emission Scanning Electron Microscopy (FESEM) and Energy-Dispersive X-ray Spectroscopy (EDX). The EDX results revealed that the membrane surface is predominantly composed of carbon (C), oxygen (O), manganese (Mn), and nickel (Ni), accounting for 22.82% by mass, whereas the cross-section analysis revealed higher mass percentages of titanium (Ti), sulphur (S), oxygen (O), carbon (C), and fluorine (F), totalling 53.51%. Tensile testing confirmed the membrane's strength, with a tensile stress of 13.71 N/mm² and an elongation at break of 73.73%. Thermal stability and breakdown behaviour were determined using Thermogravimetric Analysis (TGA), which validated this membrane thermal endurance at 422oC degradation temperatures. These findings provide significant understanding into the surface morphology and structural functional features of PFSA membranewhich allow its optimisation for advanced electrochemical applications.KeywordsPerfluorosulfonic acid (PFSA),morphology, chemical, physiochemical1.IntroductionPerfluorosulfonic acid (PFSA) membrane, employed in proton exchange membrane (PEM) fuel cells, demonstrate a distinctive set of properties essential for optimal performance in electrochemical applications[1].This membrane shows high proton conductivity, exceptional chemical and thermal stability, and mechanical strength, rendering it suitable in various applications such as fuel cells, electrolyser and redox flow batteries[2]. PFSA membranes play a crucial role in electrochemical devices, particularly in proton exchange membranes (PEMs) for fuel cells and electrolysers. Instead of that, its nanostructured morphology influences proton conductivity, mechanical strength, and chemical stability[3]. These unique design of PFSA membranes, consisting of hydrophobic polytetrafluoroethylene (PTFE) backbones and hydrophilic sulfonic acid side chains, is key to

    Quelle: Journal of Science and Technology. 17

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    MALAYSIAN JOURNAL OF CHEMISTRY (MJChem) MJChem is double-blind peer reviewed journal published by the Malaysian Institute of Chemistry (Institut Kimia Malaysia) E-ISSN: 2550-1658 About Editor Reader Author Reviewer Register Login Vol 26 No 5 (2024): Malaysian Journal of Chemistry Date Published: 21 October 2024 Antioxidant and Antibacterial Activities of Coriander (Coriander sativum L.) Seeds Essential Oil Mazlin Mohideen*, Anis Mohd Amran, Auni Farhah Azmi and Nur Azzalia Kamaruzaman 1-9Corrosion Inhibitory Evaluation of Indole-3-Carbaldehyde 4-Methyl-3-Thiosemicarbazone on Mild Steel: Weight Loss, Langmuir Isotherm, SEM-EDX and DFT Analysis Intan Syahirah Abdul Salam, Sheikh Ahmad Izaddin Sheikh Mohd Ghazali, Siti Syaida Sirat and Nur Nadia Dzulkifli* 10-22Photocatalytic Degradation of Phenol using Copper-Doped Graphitic Carbon Nitride under Fluorescent and Sunlight Irradiation Nurul Izzah Norhisan, Siti Hajar Alias*, Nur Nazzatul Azzin Ahmad Tarmizi, Siti Nor Atika Baharin, Salman Al Faridzy Akbar, Sheikh Ahmad Izaddin Sheikh Mohd Ghazali and Hadi Nur 23-33Assessment of Organobentonite’s Adsorption Kinetics for Efficient Removal of Methylene Blue Dye from Aqueous Solutions Sami Mohammad, Mohamad Nasir Mohamad Ibrahim, Sumiyyah Sabar, Rahadian Zainul*, Ida Ayu Gede Widihati, Harits Atika Ariyanta and Anwar Iqbal* 34-45Surface and Textural Analyses for Bimetallic Nickel-Based Catalyst onto Various Support using Microwave Assisted Synthesis Salma Samidin, Azizul Hakim Lahuri, Wan Nor Roslam Wan Isahak*, Khairul Naim Ahmad, Muhammad Rahimi Yusop and Norliza Dzakaria 46-55Evaluation of Different Metal-Doped ZIF-8 Through Cyclic Voltammetry for Fuel Cell Electrode Khairul Rijal Razali, Muhammad Hafiz Nor Sham, Aishah Abdul Jalil and Juan Matmin* 56-62Studies on Phytochemical and Biological Activities of Mentha piperita (Peppermint) Anis Nadira Mahat and Rohaiza Saat* 63-71Exploring SB2OME and Metal Complexes as Antibacterial Agents: Synthesis, Characterization and Molecular Docking

    Quelle: MALAYSIAN JOURNAL OF CHEMISTRY. 26

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